Publication Type:

Journal Article

Source:

Micro Nano Letters, Volume 15, Issue 12, p.817-821 (2020)

Keywords:

adsorption, chromium, chromium sorption, contact time, controlled functionalisation, direct compounding method, ethylene diamine modified graphene oxide, Fourier transform spectra, Graphene, Infrared spectra, intercalation compounds, mass 0.05 g, Monolayers, Nanocomposites, nanofabrication, one-pot synthesis approach, oxidation, pH, scanning electron microscopy, SEM-EDX techniques, Sorption, thermal analysis, time 60.0 min, X-ray chemical analysis, X-Ray Diffraction

Abstract:

Introduction of ethylene diamine into the layers of graphene oxide was achieved through direct compounding method. Graphene oxide intercalated with ethylene diamine was characterised by Fourier transform-infrared spectroscopy (FT-IR), X-ray diffraction (XRD), thermo gravimetric analysis (TGA) and scanning electron microscopy-energy dispersive X-ray spectroscopy (SEM-EDX) techniques. The efficiency of the material in adsorbing chromium was evaluated through batch scale studies by optimising parameters like pH, concentration and contact time. The material renders a monolayer adsorption capacity of 69.93 mg/g, at pH 1 within 60 min time period for a minimal dosage of 0.05 g. The ethylene diamine modified graphene oxide thus appeals to be a promising adsorbent for environmental applications.

Cite this Research Publication

G. Govindankutty, S. Hareendran, Dr. Asha Sathish, and Nithya K., “Controlled functionalisation of graphene oxide using ethylene diamine: a one-pot synthesis approach for chromium sorption”, Micro Nano Letters, vol. 15, no. 12, pp. 817-821, 2020.