Course

1. Estimation of Calcium (Permanganometry)
2. Estimation of Barium (Iodometry)
3. Estimation of Calcium as Calcium Carbonate (Gravimetry)
4. Estimation of Zinc using oxine (Gravimetry)
5. Estimation of Iron as Ferric Oxide (Gravimetry)
6. Analysis of Brass
7. Estimation of Copper and Nickel in a Mixture
8. Estimation of Copper and Iron in a Mixture
9. Preparation and Determination of Ferrous Oxalate
10. Estimation of Different Types of Hardness in the given Water Sample
11. Estimation of Different Types of Alkalinities in the given Water Sample
12. Estimation of Dissolved Oxygen in the given Water Sample
13. Complexometric Estimations
14. Analysis of some typical alloys such as brass, bronze and type metal.
15. Ion exchange methods of analysis: (i).Determination of capacity of anion exchange resin.(ii).Separation of Zinc and Magnesium on an anion exchange resin and estimation of Mg²⁺ and Zn²⁺

• CO01: Perform quantitative chemical analyses using classical wet-chemical methods such as permanganometry, complexometry, iodometry, and gravimetry to accurately estimate metal ions, hardness, alkalinity and dissolved oxygen in given samples.
• CO02: Apply separation and analysis techniques for single-component and multicomponent systems, including alloy analysis, mixed-ion estimation and ion-exchange methods, to determine composition and purity of materials.
• CO03: Demonstrate good laboratory practice and develop data analysis skills with appropriate accuracy, precision and error consideration.

Textbooks

1. Svehla, ‘Vogel’s Qualitative Inorganic Analysis’, 7^th Edition’, Prentice Hall, 1996.
2. A. Skoog and D. M. West, ‘Analytical Chemistry- An Introduction’, 4^th Edition, CBS Publishing Japan Ltd., 1986.

References

1. J. Meehan, S. Bruckenstein and I. M. Kolthoff and E. B. Sandell,‘Quantitative Chemical Analysis’, 4^th Edition, The Macmillan Company, 1969.
2. A. Day (Jr) and A. L. Underwood,’ Quantitative Analysis’, 6^th Edition, Prentice Hall of India, 1991.