Course

Syllabus

Experiments:

1. Preparation of benzopinacolone (pinacol-pinacolone rearrangement).
2. Addition of Ethyl Acetoacetate to Chalcone (Michael addition).
3. Oxidation of cyclohexanol to cyclohexanone.
4. Preparation of quinoline.
5. Preparation of 2-phenyl indole.
6. Synthesis of anisole from phenol.
7. Conversion of a low sweet glucose to a high sweet fructose.
8. Preparation of 2-phenyl indole (fischer indole synthesis).
9. Preparation of methyl orange from sulphonilic acid.
10. Isolation of caffeine from tea leaves.
11. Isolation of lactose from milk.
12. Isolation of β-carotene from carrots.
13. Isolation of piperine from black pepper.

Text Books / References

Reference

1. Vogel. (1989). Textbook of Practical Organic Chemistry, Fifth edition, Longman Scientific & Technical, London, England.
2. J. N. Gurtu and R. Kapoor. (1982). Advanced Experimental Chemistry, S. Chand & Company Limited, New Delhi-55, India.
3. O. P. Agarwal. (2000). Practical Organic Chemistry, Goel Publishing House, Meerut, India.
4. E. Fisher. (1909). Introduction to the preparation of organic compounds, 108-109.
5. Clarke, H.T. (1975). A Handbook of Organic. Analysis Qualitative and Quantitative. Edward Arnold Publishers Ltd London.
6. Vogel, A.I., Tatchell, A.R., Furnis, B.S., Hannaford, A.J., Smith, P.W.G. (1996). Textbook of Practical Organic Chemistry. Prentice-Hall

Course Outcome:

• CO1: To perform organic reactions involving rearrangement, condensation, cyclization, isomerization, and azo coupling using standard laboratory techniques.
• CO2: To explain the underlying mechanisms of the transformations carried out during the experiments.
• CO3: To purify, isolate, and calculate yields of the synthesized organic products using appropriate laboratory methods.
• CO4: To analyze and interpret spectroscopic data obtained to confirm the structure and purity of synthesized compounds.

CO-PO Mapping: