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Microstructural evaluation and optimization of wear behaviour of vacuum arc melted AlFeCrNiSi high entropy alloy

Publication Type : Journal Article

Publisher : Elsevier BV

Source : Materials Today Communications

Url : https://doi.org/10.1016/j.mtcomm.2024.110594

Keywords : High entropy alloy, Vacuum arc melting, Microstructure, Wear resistance, Taguchi optimization

Campus : Chennai

School : School of Engineering

Department : Mechanical Engineering

Year : 2024

Abstract : High-entropy alloys (HEA) are equiatomic, multi-element systems that, while having several elements with various crystal geometries to form a single phase. In this study, a novel equiatomic AlFeCrNiSi HEA is prepared using the vacuum arc melting process. The resulting microstructure featured dendritic and inter-dendritic structures with formations of intermetallic compounds such as Al₃Fe₂Si, NiAl, and AlCrNi phases. EDS analysis confirmed the presence of alloying elements and EBSD analysis revealed refined grains with an average size of 1 ± 0.15 µm size. Pin-on-Disc wear test with varying test parameters is conducted to optimize the wear parameters. Signal-to-noise ratio and analysis of variance identified the most significant wear parameters, with load being the most influential, followed by sliding distance and velocity. The wear rate is minimum at the lowest conditions of applied load, sliding distance, and sliding velocity. The improved microhardness also contributed to the improved wear resistance of the cast alloy. The subsequent worn morphology revealed the formation of grooves, microcracks, and oxide layers on the worn surface.

Cite this Research Publication : N. Radhika, M.V. Kamal, V. Ram Srivatsav, M. Sathishkumar, T. Ramkumar, Microstructural evaluation and optimization of wear behaviour of vacuum arc melted AlFeCrNiSi high entropy alloy, Materials Today Communications, Elsevier BV, 2024, https://doi.org/10.1016/j.mtcomm.2024.110594

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